PPL Inside Chamber for Hydrothermal Synthesis Autoclave Reactors, Volume:100ml

Technical Specification:

1. Material Composition:
   • Material: Polyphenylene (PPL).
     • Renowned for its superior chemical resistance and thermal stability, particularly in extreme environments where PTFE liners may fail.
2. Physical Dimensions:
   • Volume: 100 mL.
     • Designed to fit perfectly within standard 100 mL hydrothermal synthesis autoclave reactors.
   • Wall Thickness: Typically 2–5 mm, ensuring robust protection and structural stability under high pressure.
   • Height and Diameter: Precisely engineered to match the internal dimensions of the autoclave.
3. Thermal Properties:
   • Maximum Operating Temperature: 280°C
     • Higher thermal tolerance compared to PTFE liners, making it suitable for reactions under elevated conditions.
   • Thermal Stability:
     • Maintains performance across a wide range of reaction temperatures.
4. Mechanical Properties:
   • Pressure Resistance: Supports pressures up to 3 MPa (30 bar), depending on the reactor design.
   • Durability: Built to withstand multiple reaction cycles without degradation.
5. Chemical Resistance:
   • Inertness:
     • Resistant to aggressive chemicals, including strong acids (e.g., HCl, H₂SO₄), strong bases (e.g., NaOH), and organic solvents.
   • Non-Contaminating:
     • Maintains the purity of reactions by preventing chemical interactions.
6. Ease of Use:
   • Non-Stick Surface:
     • Ensures easy cleaning and reduces the accumulation of residues.
   • Insertable Design:
     • Simple to insert and remove from the autoclave reactor shell.

Applications:

1. Primary Applications:
   • Reaction Vessel Liner:
     • Acts as a chemically resistant barrier to contain reactants and solvents during hydrothermal or solvothermal synthesis.
2. Industries:
   • Material Science:
     • Enables the synthesis of nanomaterials, crystals, and advanced materials.
   • Chemical Research:
     • Facilitates high-pressure, high-temperature reaction studies.
   • Pharmaceuticals:
     • Suitable for the crystallization of high-purity compounds.
   • Geology:
     • Used to replicate hydrothermal conditions for mineral and crystal growth.
3. Advantages for Applications:
   • Chemical Compatibility:
     • Suitable for reactions involving aggressive chemicals and high acidity.
   • High Thermal Tolerance:
     • Can handle elevated temperatures up to 280°C, expanding the range of reactions.
   • Durability:
     • Designed for long-term use with minimal maintenance requirements.
   • Compact and Efficient:
     • A convenient size for laboratory-scale experiments.
4. Specialized Uses:
   • Nanotechnology:
     • Facilitates the growth of nanostructures like nanowires, graphene oxide, and carbon nanotubes.
   • Catalyst Development:
     • Supports the preparation of advanced catalytic materials for research and industry.
   • Experimental Research:
     • Enables detailed studies on reaction mechanisms, kinetics, and material behavior.
5. Challenges and Mitigation:
   • Volume Limitations:
     • Restricted to 100 mL reaction capacity.
       • Solution: Ideal for medium-scale research; scale up with larger reactors for production.
   • Handling and Maintenance:
     • PPL is more delicate than stainless steel and requires careful handling.
       • Solution: Use non-abrasive tools and gentle cleaning methods.
   • Temperature Constraints:
     • Exceeding 280°C may damage the liner.
       • Solution: Operate within the recommended temperature range for optimal performance.

Summary:

The PPL Inside Chamber for Hydrothermal Synthesis Autoclave Reactors (100 mL) is a durable and versatile solution for conducting high-temperature, high-pressure reactions. Its exceptional chemical resistance and thermal stability make it an ideal choice for material synthesis, nanotechnology, and chemical research. Proper use and maintenance ensure consistent performance and long-term reliability in demanding laboratory environments.