Hydrothermal Synthesis Autoclave Reactor with PTFE Lined Vessel 100 ml

Technical Specification:

1. Material Composition:
   • Outer Shell: High-strength stainless steel (typically 304SS or 316SS).
     • Provides excellent corrosion resistance, durability, and pressure tolerance.
   • Inner Liner: PTFE (Polytetrafluoroethylene).
     • Chemically inert, heat-resistant material that prevents reactions between chemicals and the stainless steel body.
2. Physical Dimensions:
   • Vessel Capacity: 100 mL.
     • Accommodates medium-scale experimental reactions.
   • Outer Dimensions:
     • Compact, typically 15–20 cm in height, depending on manufacturer design.
   • Weight: 1.5–3 kg, depending on build and specifications.
3. Temperature and Pressure Ratings:
   • Maximum Temperature: 240°C
   • Maximum Pressure: 3 MPa (30bar), suitable for most hydrothermal and solvothermal processes.
4. Sealing Mechanism:
   • High-strength threaded closure with a gasket or O-ring ensures airtight sealing to withstand high pressures.
   • PTFE liner eliminates direct contact between the reactants and the metal body.
5. Safety Features:
   • Pressure Relief Mechanism:
     • Equipped with vents or safety valves to release excess pressure when needed.
   • Thermal Stability:
     • Both the PTFE liner and stainless steel shell withstand high-temperature fluctuations.
6. Accessories and Packaging:
   • Includes necessary tools such as wrenches for sealing, spare gaskets, and an operation manual.

Applications:

1. Primary Applications:
   • Hydrothermal Synthesis:
     • Preparation of nanomaterials, crystalline materials, and other advanced compounds under controlled high-pressure and high-temperature conditions.
   • Solvothermal Reactions:
     • Ideal for reactions in organic solvents at elevated temperatures and pressures.
2. Industries:
   • Material Science:
     • Fabricating nanoparticles, nanowires, and functional materials for advanced applications.
   • Chemical Research:
     • Synthesis of new compounds and reaction mechanisms at extreme conditions.
   • Geology:
     • Simulation of natural geological processes to synthesize minerals or mimic hydrothermal environments.
   • Pharmaceuticals:
     • Crystallization and preparation of high-purity substances.
3. Advantages for Applications:
   • Chemical Compatibility:
     • PTFE liner ensures safe handling of highly reactive or corrosive chemicals.
   • High-Pressure Capability:
     • Enables reactions that require extreme conditions for material transformation.
   • Medium Capacity:
     • 100 mL volume balances scalability and efficiency for research purposes.
   • Ease of Use:
     • Compact design and safety features make it suitable for laboratory use.
4. Specialized Uses:
   • Nanotechnology:
     • Growth of nanocrystals, graphene, and carbon nanotubes.
   • Catalyst Synthesis:
     • Preparation of catalytic materials for chemical and industrial applications.
   • Experimental Studies:
     • Investigation of reaction kinetics, crystal growth, and material behaviors under hydrothermal conditions.
5. Challenges and Mitigation:
   • Pressure Risks:
     • Overpressure can compromise safety.
       • Solution: Operate within recommended temperature and pressure limits and use pressure-relief systems.
   • Maintenance:
     • PTFE liners may degrade over time with repeated use.
       • Solution: Inspect and replace liners as necessary.
   • Scale Limitation:
     • Limited to 100 mL per reaction.
       • Solution: Use larger reactors for industrial-scale applications after laboratory trials.

Summary:

The Hydrothermal Synthesis Autoclave Reactor with PTFE Lined Vessel (100 mL) is a reliable and versatile tool for conducting high-pressure and high-temperature reactions. Its chemical inertness, robust construction, and compact design make it ideal for material synthesis, nanotechnology, and chemical research. The 100 mL capacity supports medium-scale experiments while maintaining laboratory efficiency and safety.