Hydrothermal Synthesis Autoclave Reactor with PPL Lined Vessel 50 ml

Technical Specification:

1. Material Composition:
   • Outer Shell: High-strength stainless steel (commonly 304SS or 316SS).
     • Provides excellent resistance to pressure, corrosion, and thermal stress.
   • Inner Liner: Polyphenylene (PPL).
     • Highly resistant to extreme chemical environments, outperforming PTFE in certain high-temperature and highly acidic conditions.
2. Physical Dimensions:
   • Vessel Volume: 50 mL.
     • Suitable for small-scale synthesis and laboratory experiments.
   • Wall Thickness (PPL Liner): Typically 2–5 mm, ensuring durability under extreme conditions.
   • Outer Dimensions:
     • Compact design optimized for laboratory use.
3. Thermal and Pressure Ratings:
   • Maximum Operating Temperature: 280°C–300°C (higher than PTFE-lined vessels).
   • Maximum Pressure: 10 MPa (100 bar), allowing for high-pressure reactions.
   • Thermal Stability:
     • Excellent resistance to temperature fluctuations.
4. Sealing Mechanism:
   • High-strength threaded closure with a durable gasket or O-ring for airtight sealing.
   • PPL liner isolates the reactants from the stainless steel body, ensuring compatibility with aggressive chemicals.
5. Chemical Resistance:
   • Exceptional Resistance:
     • Handles highly acidic and alkaline solutions, making it suitable for aggressive chemical reactions.
   • Non-Contaminating:
     • Ensures pure reaction environments.
6. Packaging:
   • Supplied with necessary accessories, including wrenches for sealing, spare gaskets, and a user manual.

Applications:

1. Primary Applications:
   • Hydrothermal Synthesis:
     • Ideal for the preparation of nanomaterials, advanced crystals, and other functional materials in a high-pressure, high-temperature environment.
   • Solvothermal Reactions:
     • Facilitates reactions in organic solvents under elevated conditions.
2. Industries:
   • Material Science:
     • Enables the synthesis of nanomaterials, graphene, and functional composites.
   • Chemical Research:
     • Supports high-pressure, high-temperature reaction studies.
   • Geology:
     • Simulates natural geological processes to grow minerals and crystals.
   • Pharmaceuticals:
     • Suitable for the crystallization and synthesis of high-purity substances.
3. Advantages for Applications:
   • Higher Temperature Tolerance:
     • PPL liners can withstand temperatures up to 300°C, making them ideal for reactions requiring elevated heat.
   • Improved Chemical Resistance:
     • Superior to PTFE in resisting highly acidic and oxidative environments.
   • Compact Size:
     • Perfect for small-scale research and exploratory experiments.
   • Safety:
     • Designed with safety features to handle extreme conditions.
4. Specialized Uses:
   • Nanotechnology:
     • Growth of nanowires, nanocrystals, and other advanced structures.
   • Catalyst Synthesis:
     • Creation of high-performance catalysts for industrial and research applications.
   • Experimental Research:
     • Supports reaction mechanism studies under extreme conditions.
5. Challenges and Mitigation:
   • Limited Volume:
     • 50 mL capacity may be insufficient for larger-scale experiments.
       • Solution: Use for R&D and scale up with larger reactors for production.
   • Temperature Management:
     • While PPL offers higher tolerance than PTFE, it still has thermal limits.
       • Solution: Monitor and control temperature to avoid exceeding the safe range.
   • Liner Durability:
     • PPL liners require careful handling to prevent scratches or damage.
       • Solution: Handle gently and use non-abrasive tools for cleaning.

Summary:

The Hydrothermal Synthesis Autoclave Reactor with PPL Lined Vessel (50 mL) is a highly versatile tool for conducting high-temperature and high-pressure reactions. Its superior chemical and thermal resistance make it ideal for advanced material synthesis, nanotechnology, and experimental research. The small volume is perfect for laboratory-scale applications, offering reliable and efficient performance under extreme conditions.