Hydrothermal Synthesis Autoclave Reactor with PTFE Lined Vessel 50 ml

Technical Specification:

1. Material Composition:
   • Outer Shell: High-quality stainless steel (commonly 304SS or 316SS).
     • Provides excellent durability, pressure resistance, and corrosion protection.
   • Inner Liner: PTFE (Polytetrafluoroethylene).
     • Chemically inert and heat-resistant material to contain reactive substances safely.
2. Physical Dimensions:
   • Vessel Capacity: 50 mL.
     • Suitable for small-scale laboratory synthesis.
   • Outer Dimensions:
     • Varies slightly by manufacturer; typically compact for easy handling and storage.
   • Weight: Approximately 1–2 kg, depending on design.
3. Temperature and Pressure Ratings:
   • Maximum Temperature: 220°C–250°C (depending on PTFE liner specification).
   • Maximum Pressure: 3–6 MPa (30–60 bar), ensuring safe operation under hydrothermal conditions.
4. Sealing Mechanism:
   • High-strength threaded closure with a gasket or O-ring to ensure airtight sealing and prevent leaks.
   • PTFE liner prevents direct contact between the stainless steel shell and the reactants.
5. Safety Features:
   • Pressure Relief Mechanism:
     • Built-in safety features (e.g., pressure vents) to release excess pressure if necessary.
   • Thermal Resistance:
     • PTFE and stainless steel resist thermal stress and chemical corrosion.
6. Packaging:
   • Delivered with accessories such as a wrench for closure, gaskets, and a user manual.

Applications:

1. Primary Applications:
   • Hydrothermal Synthesis:
     • Used for preparing nanomaterials, crystals, and other advanced materials under high-pressure and high-temperature conditions.
   • Material Research:
     • Essential in chemical synthesis, mineral digestion, and hydrothermal growth experiments.
2. Industries:
   • Material Science:
     • Synthesizing nanoparticles, nanowires, and other functional materials.
   • Chemical Engineering:
     • Reaction studies involving superheated water or solvothermal processes.
   • Geology:
     • Mimicking natural geological processes for mineral synthesis.
   • Pharmaceuticals:
     • Developing novel compounds or crystallization processes.
3. Advantages for Applications:
   • Chemical Inertness:
     • PTFE liner ensures compatibility with strong acids, bases, and organic solvents.
   • Temperature and Pressure Resistance:
     • Enables reactions requiring extreme conditions for material synthesis.
   • Compact Design:
     • Ideal for laboratory use and small-batch research.
   • Safety and Reliability:
     • Designed to handle high-pressure conditions with robust safety mechanisms.
4. Specialized Uses:
   • Nanomaterial Synthesis:
     • Growth of high-purity crystals, graphene oxide, and carbon dots.
   • Hydrothermal Treatment:
     • Processing waste materials or developing catalytic supports.
   • Experimental Research:
     • Study of high-temperature and high-pressure reaction kinetics and mechanisms.
5. Challenges and Mitigation:
   • Limited Capacity:
     • 50 mL may be insufficient for larger-scale experiments.
       • Solution: Use larger-capacity reactors or scale up after successful trials.
   • Pressure Risks:
     • Overpressure can lead to safety concerns.
       • Solution: Always operate within specified pressure and temperature limits.
   • PTFE Liner Maintenance:
     • PTFE liners can degrade under harsh conditions over time.
       • Solution: Inspect regularly and replace liners as needed.

Summary:

The Hydrothermal Synthesis Autoclave Reactor with PTFE Lined Vessel (50 mL) is a compact and versatile tool for conducting high-temperature and high-pressure reactions in research and development settings. Its chemical inertness, robust construction, and precise sealing make it indispensable for material synthesis, nanotechnology, and advanced chemical studies. Proper use and maintenance ensure safe and reliable operation.